Preparations and spectroscopic studies of organotin complexes of diclofenac
| dc.contributor.author | Kourkoumelis, N. | en |
| dc.contributor.author | Demertzis, M. A. | en |
| dc.contributor.author | Kovala-Demertzi, D. | en |
| dc.contributor.author | Koutsodimou, A. | en |
| dc.contributor.author | Moukarika, A. | en |
| dc.date.accessioned | 2015-11-24T16:45:30Z | |
| dc.date.available | 2015-11-24T16:45:30Z | |
| dc.identifier.issn | 1386-1425 | - |
| dc.identifier.uri | https://olympias.lib.uoi.gr/jspui/handle/123456789/8942 | |
| dc.rights | Default Licence | - |
| dc.subject | vibrational spectra | en |
| dc.subject | nmr and mossbauer spectra | en |
| dc.subject | diclofenac acid | en |
| dc.subject | organotin complexes | en |
| dc.subject | state c-13 nmr | en |
| dc.subject | molecular-structure | en |
| dc.subject | diorganotin derivatives | en |
| dc.subject | methyltin(iv) compounds | en |
| dc.subject | crystal | en |
| dc.subject | adducts | en |
| dc.subject | angle | en |
| dc.subject | acid | en |
| dc.title | Preparations and spectroscopic studies of organotin complexes of diclofenac | en |
| heal.abstract | The reactions of the potent and widely used anti-inflammatory drug diclofenac, HL,with diorganotin(IV) oxides were studied. The dimeric tetraorganodistannoxane complexes [Me2LSnOSnLMe2](2), [Bu2LSnOSnLBu2](2), [Ph2LSnOSnLPh2](2) and the dibutyltin complex [Bu2SnL2], have been prepared and structurally characterized in the solid state by means of vibrational and Sn-119 Mossbauer spectroscopy. Determination of lattice dynamics by temperature-dependent Sn-119 Mossbauer spectroscopy. From the variable-temperature Mossbauer effect, the Debye temperature was determined. The complexes have been characterized in solution by NMR (H-1 and C-13) spectroscopy. Vibrational, Mossbauer, and NMR data are discussed in terms of the proposed structures. (C) 2003 Elsevier B.V. All rights reserved. | en |
| heal.access | campus | - |
| heal.fullTextAvailability | TRUE | - |
| heal.identifier.primary | DOI 10.1016/j.saa.2003.11.027 | - |
| heal.identifier.secondary | <Go to ISI>://000223065100010 | - |
| heal.identifier.secondary | http://ac.els-cdn.com/S1386142503005511/1-s2.0-S1386142503005511-main.pdf?_tid=ec4fc15581934ce64a3ceee3acf1133e&acdnat=1333028638_ee15d50e358568079678ac23bf85a650 | - |
| heal.journalName | Spectrochimica Acta Part a-Molecular and Biomolecular Spectroscopy | en |
| heal.journalType | peer reviewed | - |
| heal.language | en | - |
| heal.publicationDate | 2004 | - |
| heal.recordProvider | Πανεπιστήμιο Ιωαννίνων. Σχολή Θετικών Επιστημών. Τμήμα Χημείας | el |
| heal.type | journalArticle | - |
| heal.type.el | Άρθρο Περιοδικού | el |
| heal.type.en | Journal article | en |
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