Determination of residues of UV filters in natural waters by solid-phase extraction coupled to liquid chromatography-photodiode array detection and gas chromatography-mass spectrometry

dc.contributor.authorGiokas, D. L.en
dc.contributor.authorSakkas, V. A.en
dc.contributor.authorAlbanis, T. A.en
dc.date.accessioned2015-11-24T16:55:45Z
dc.date.available2015-11-24T16:55:45Z
dc.identifier.issn0021-9673-
dc.identifier.urihttps://olympias.lib.uoi.gr/jspui/handle/123456789/10352
dc.rightsDefault Licence-
dc.subjectwater analysisen
dc.subjectsolid-phase extractionen
dc.subjectsunscreen agentsen
dc.subjectsunscreen agentsen
dc.subjectproductsen
dc.titleDetermination of residues of UV filters in natural waters by solid-phase extraction coupled to liquid chromatography-photodiode array detection and gas chromatography-mass spectrometryen
heal.abstractThis study describes a procedure for the enrichment, separation and quantification of four major UV filters in natural waters. Solid-phase extraction combined with liquid chromatography and photodiode array detection (LC-UV-DAD), and gas chromatography with mass spectroscopy (GC-MS) were employed for the analyses. LC of the four compounds with surfactant-modified hydro-organic eluents gave satisfactory resolution of overlapping peaks. In GC, a significant improvement of the detection limits was attained, but only three compounds could be detected. The method was validated for, and applied to, various water samples prone to UV filter accumulation due to recreational activities. Recoveries from real samples were 86-99% with LOQs as low as 0.5 ng/l depending on the sample volume and the analytical procedure. (C) 2003 Elsevier B.V. All rights reserved.en
heal.accesscampus-
heal.fullTextAvailabilityTRUE-
heal.identifier.primaryDOI 10.1016/j.chroma.2003.10.114-
heal.identifier.secondary<Go to ISI>://000188200300032-
heal.identifier.secondaryhttp://ac.els-cdn.com/S0021967303020119/1-s2.0-S0021967303020119-main.pdf?_tid=f6af8a6e-349c-11e3-bce6-00000aacb35f&acdnat=1381733631_c7366158dadbac2a6cb3542a62a2457e-
heal.journalNameJournal of Chromatography Aen
heal.journalTypepeer reviewed-
heal.languageen-
heal.publicationDate2004-
heal.publisherElsevieren
heal.recordProviderΠανεπιστήμιο Ιωαννίνων. Σχολή Θετικών Επιστημών. Τμήμα Χημείαςel
heal.typejournalArticle-
heal.type.elΆρθρο Περιοδικούel
heal.type.enJournal articleen

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