Organotin adducts of indomethacin: synthesis, crystal structures and spectral characterization of the first organotin complexes of indomethacin

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dc.contributor.authorGalani, A.en
dc.contributor.authorKovala-Demertzi, D.en
dc.contributor.authorKourkoumelis, N.en
dc.contributor.authorKoutsodimou, A.en
dc.contributor.authorDokorou, V.en
dc.contributor.authorCiunik, Z.en
dc.contributor.authorRusso, U.en
dc.contributor.authorDemertzis, M. A.en
dc.date.accessioned2015-11-24T16:43:34Z
dc.date.available2015-11-24T16:43:34Z
dc.identifier.issn0277-5387-
dc.identifier.urihttps://olympias.lib.uoi.gr/jspui/handle/123456789/8715
dc.rightsDefault Licence-
dc.subjectindomethacinen
dc.subjectdiorganotinen
dc.subjectcrystal structuresen
dc.subjectspectroscopic studiesen
dc.subjectnonsteroidal antiinflammatory drugsen
dc.subjectmolecular-structureen
dc.subjectdiorganotin derivativesen
dc.subjectmefenamic-aciden
dc.subjectin-vitroen
dc.subjectagentsen
dc.subjecth-1en
dc.subjectnmren
dc.titleOrganotin adducts of indomethacin: synthesis, crystal structures and spectral characterization of the first organotin complexes of indomethacinen
heal.abstractThe complexes [Me-2(Indo)SnOSn(Indo)Me-2](2), (1) [Bu-2(Indo)SnOSn(Indo)Bu-2](2), (2), where Hindo is indomethacin, have been prepared and structurally characterized by means of Sn-119 Mossbauer, vibrational, and NMR (H-1 and C-13) spectroscopy. The crystal structures of the complexes [Me-2(Indo)SnOSn(Indo)Me-2](2) (.) 2C(4)H(8)O(2), 3 and 2 have been determined by X-ray crystallography. Each structure is centro-symmetric and features a central rhombus Sn2O2 unit with two additional tin atoms linked at the O atoms. Pairs of tin atoms are bridged by bidentate carboxylate ligands and by a monoatomic bridging oxygen. C-H --> pi, pi --> pi, stacking interactions, inter and intramolecular hydrogen bonds stabilize the structures 2 and 3. Complexes 2 and 3 are self-assembled via pi --> pi. C-H-pi and stacking interactions. (C) 2004 Elsevier Ltd. All rights reserved.en
heal.accesscampus-
heal.fullTextAvailabilityTRUE-
heal.identifier.primaryDOI 10.1016/j.poly.2004.05.004-
heal.identifier.secondary<Go to ISI>://000222977000023-
heal.identifier.secondaryhttp://ac.els-cdn.com/S0277538704001962/1-s2.0-S0277538704001962-main.pdf?_tid=f9169e9aa897c3f605455c3b6db6472d&acdnat=1333028548_1f5bd237e4c5f756383365a9f76d36a5-
heal.journalNamePolyhedronen
heal.journalTypepeer reviewed-
heal.languageen-
heal.publicationDate2004-
heal.recordProviderΠανεπιστήμιο Ιωαννίνων. Σχολή Θετικών Επιστημών. Τμήμα Χημείαςel
heal.typejournalArticle-
heal.type.elΆρθρο Περιοδικούel
heal.type.enJournal articleen

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