Nanostructure and bimodal structure of Si3N4 ceramics developed by spark plasma sintering method

dc.contributor.authorFu, R. L.en
dc.contributor.authorAgathopoulos, S.en
dc.date.accessioned2015-11-24T17:36:25Z
dc.date.available2015-11-24T17:36:25Z
dc.identifier.issn1743-6753-
dc.identifier.urihttps://olympias.lib.uoi.gr/jspui/handle/123456789/14245
dc.rightsDefault Licence-
dc.subjectsi3n4en
dc.subjectmicrostructureen
dc.subjectmechanical propertiesen
dc.subjectgrain sizeen
dc.subjectsinteringen
dc.subjectnanoceramicsen
dc.subjectsilicon-nitride ceramicsen
dc.subjectabnormal grain-growthen
dc.subjecthot-pressed si3n4en
dc.subjectmicrostructureen
dc.subjectenergyen
dc.subjectfabricationen
dc.subjectcompositeen
dc.subjectstrengthen
dc.subjectsialonen
dc.titleNanostructure and bimodal structure of Si3N4 ceramics developed by spark plasma sintering methoden
heal.abstractThe densification of high energy ball milled Si3N4 nanopowders through spark plasma sintering was investigated. Nanoceramics of Si3N4, with fine microstructure, comprising of grains with a diameter of similar to 70 nm, were produced after sintering at 1600 degrees C for 5 min in N-2 atmosphere with a fast heating rate of 300 K min(-1). The size and the aspect ratio of Si3N4 grains increased with decreasing heating rate and increasing holding time and temperature. Post-annealing of sintered ceramics at 1850 degrees C for 3 h favoured development of a self-reinforced bimodal microstructure containing large elongated grains.en
heal.accesscampus-
heal.fullTextAvailabilityTRUE-
heal.identifier.primaryDoi 10.1179/174367609x413973-
heal.identifier.secondary<Go to ISI>://000268849000006-
heal.journalNameAdvances in Applied Ceramicsen
heal.journalTypepeer reviewed-
heal.languageen-
heal.publicationDate2009-
heal.publisherManey Publishingen
heal.recordProviderΠανεπιστήμιο Ιωαννίνων. Σχολή Θετικών Επιστημών. Τμήμα Μηχανικών Επιστήμης Υλικώνel
heal.typejournalArticle-
heal.type.elΆρθρο Περιοδικούel
heal.type.enJournal articleen

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